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1200w Direct Injection Sampling Inductively Coupled Plasma Emission Spectrometer Icp-6800s

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Macylab Instruments Inc.

1200w Direct Injection Sampling Inductively Coupled Plasma Emission Spectrometer Icp-6800s

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Product Details

                               Inductively Coupled Plasma Optical Emission Spectrometer ICP-6800S                            

 

   

    Petrochemical Inductively Coupled Plasma Optical Emission Spectrometer(ICP6800S) is a professional instrument for the petrochemical industry launched by Macylab Instruments. It can be used to determine more than 30 elements in crude oil, mainly for Fe, Na, Mg, Ni, V, Ca, Pb, Mo, Mn, Cr, Ca, Ba, As; also can be used to measure Fe, Mg, Pb, Siin gasoline ,and the wear elements of additive in lubricating oil, it also can be applied for multielement determination in base oils; for the determination of sodium in formaldehyde and the determination of oil field tracer.

 

Main features


Performance stability

The use of all-solid-state rf power supply, with small size, high efficiency, stable output power, with a variety of protection functions and many other advantages, the load using fully automatic matching technology, matching speed, improve the efficiency of the use of power supply and the stability of the instrument, and make the whole ignition process simple and convenient.

 

Injection automation

Adopting four-channel automatic design, the rotational speed can be set up according to the test demand to adjust the flow rate, carrier gas, plasma gas, auxiliary gas are all controlled by advanced mass flow controller, at the same time can be equipped with imported high salt nebulizer, imported hydrofluoric nebulizer and so on to meet the customer's various test needs.

 

Precision analysis

The middle step grating prism cross dispersion mode is adopted, there is no moving optical element, the ultra low stray light design is combined with the unique optical design, nitrogen distributed blowing, imported optical elements, intelligent and accurate automatic wavelength calibration algorithm.

 

Quick test

In American thermoelectric CID detector, the 160-1000nm range is continuously covered, and the intensity integral values of all analytical spectral lines are read out at one exposure to speed up the analysis.


 

 

Technical parameters

 

RFPower technical parameter

 

Circuit type

solid-state RF Power supply, with function of automatch

Frequercy

27.12MHz±0.05%

Frequency Stablity

<0.1%

Power Output

800W-1500W

Power Output Stability

<0.3%

Escaped RF radiation

30cm away from the instrument, electric fiekd: E<2Vtm

Sampling System Technical Parameter

 

Output working coil imer diameter

25mm

Torpue tube

Three concentric, extemal diameter 20mm

Coaxial nebulizer

Outer dameter 6mm

Double barrel atomizing chamber

Outer diameter 34mm

 

Gas Flow Controls

 

Plasma Argon Flowmeter

(100-1000)L/h(1.6-16L/min)

Auxiliary Argon Fiowmeter

(100-1000)L/h(0.16-1.6L/min)

Auxiliary Carrier Argon Flowmeter

(100-1000)L/h(0.16-1.6L/min)

Pressune Maintaining Value

(0-0.4MPa)

Cooling Water:Temperature

20-25ºC,Rate of Flow>5L/min,Hydraulic Pressure>0.1MPa

 

Spectrometer

 

Optics

Czerny-Turner type

Focal length

1000 mm

Grating

Ion Beam Etching Holographic Grating, 3600L/mm or 2400L/mm

Reciprocal linear dispersion

0.26nm/mm

Resolution

≤0.007nm(3600 line grating); ≤0.015nm(2400 line grating)

Wavelength range

3600 line grating:(190nm~500) nm; 2400 line grating:(190nm~800) nm

Minimum pace of stepping motor

≤0.0006 nm

Exit Slit

12μm

Entrance Slit

10μm

 

Photoelectric Converter Performance

 

Photomultiplier tube specification

R293/R928

Negative HV on PMT

0-1000V

Stability

<0.05%

 

Direct injection sampling and measure iron(Fe), manganese(Mn), lead(Pb) and silicon(Si) in gasoline.Analysis results:

ElementFeMnPbSi
Determination value/(mg/L)3.617.51.82.4
RSD/%0.560.231.380.92


Standard Addition Recovery Rate:

NumberStandard Addition
(mg/L)
FeMnPbSi
  Determination value(mg/L)Recovery
/%
Determination value(mg/L)Recovery
/%
Determination value(mg/L)Recovery
/%
Determination value(mg/L)Recovery
/%
10.450.43696.90.468104.00.43296.00.465103.3
20.90.88798.60.913101.40.86896.40.919102.1

   

          


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                                                                   Company profile                                                                                     

   

Macy(China) Instruments Inc is part of Shanghai Macylab Instrument Inc, is a high-tech enterprise with independent intellectual property rights . Macy hold the pioneering concept "technology - because you change " , and as a business purpose, and constantly explore, bold innovation. Especially in the field of analytical instruments ,Macy constantly develop advanced products that enable Macy to become a high-quality instrument resource supplier and leader.

 

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