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Inert gas glove box ensures water oxygen content ≤0.1ppm and leakage rate ≤ 0.001%vol /h

Hefei Jiusheng Electromechanical Technology Co., Ltd

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Address: Jiusheng Technology, Baihua Industrial Community, Wushan Town, Changfeng County, Hefei Province, Anhui Province

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Inert gas glove box ensures water oxygen content ≤0.1ppm and leakage rate ≤ 0.001%vol /h

Country/Region china
City & Province hefei anhui
Categories Pharmaceutical Machinery
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Product Details

Operating Principle:

The box and the gas purification system form a sealed working environment, and the gas in the box is continuously purified (mainly removing water and oxygen) through the gas purification system, so that the system always maintains a high clean and high purity inert gas environment. In such an environment, many experiments and production can be carried out that are not possible under normal conditions.

Application Area:

Mainly for organometrical chemistry, organic synthesis, hydrophilic chemical treatment, medical devices, electronic component treatment, lithium battery treatment, solar cell assembly, hemoglobin and metabolic research, catalyst treatment, pharmaceutical synthesis, nuclear industry, membrane industry and so on to create an oxygen-free and moist-free environment.  

Selling Point Of A Product

 
  • 1. Standard high-efficiency water and oxygen purification system: large-capacity professional-grade water and oxygen purification column adsorption system can quickly purify the experimental environment inside the glove box. Under standard conditions, that is, 20° constant temperature, a standard atmospheric pressure, relative humidity 65%, 99.999% inert air source, water oxygen index is less than 1 ppm, and under normal circumstances, water oxygen index can reach less than 0.1 ppm;
  • 2. the front door can be opened all glass front window: the maximum convenience for the operator to take the enlarged object at any time;
  • 3. Automatic pumping and replenishment of Qigong in the large transition bin: The operator can choose manual point control or automatic control according to the touch screen prompts for pumping and replenishment of Qigong in the large transition bin;
  • 4.adjustable built-in tray: the operator can adjust the height of the tray up and down according to actual needs;
  •  
  • 5. water, oxygen regeneration purification system to increase temperature control;
  • 5.1 Timely and effectively ensure the optimal reduction temperature of water and oxygen recycled materials to achieve the best purification and adsorption of water and oxygen;
  • 5.2 Greatly extend the service life of water and oxygen recycled materials;
  •  
  • 6. a full set of standard high-efficiency high-vacuum KF bellows fast interface;
  • 6.1 High precision and fast KF bellows are used for high pressure pipe connection, with high air tightness and basically no leakage problem. Customers can connect, repair and replace by themselves;
  •  
  • 7.the electrical control cabinet adopts: independent separate movable structure;
  • 7.1. the electrical components are integrated into the independent control cabinet, can be moved freely, and maintenance and replacement of spare parts are simple. Customers can repair and replace by themselves;
  • 7.2.easy to observe the direction of the gas pipeline, the use of high precision and fast KF high-pressure pipeline connection, high air tightness, basically no leakage problem. Customers can connect, repair and replace by themselves.
  • 7.3. labor cost, after-sales service, low maintenance cost;
  • 7.4. the internal space is reasonable, can install large capacity adsorption materials and a variety of functional adsorption cylinder accessories;
  • 7.5. It is a regular standby product with fast delivery rate and high cost performance;
  •  
  • 8. The organic solvent adsorption system is configured for the customized project, as shown in the diagram for the integration of air filtration and organic solvent materials;
  • 8.1. replacement and installation are simple, customers can replace themselves, easy to see the adsorption material color, to determine whether to replace, the glove box does not need to stop working;
  • 8.2. Low labor cost, processing cost, after-sales service and maintenance cost;
  • 8.3. small size, basically does not take up space, can be superimposed;
  • 8.4. the weight of the adsorption material can be changed, each independent chamber can be loaded with 1.3-1.5Kg adsorption material;
  • 8.5. directly participate in the gas cycle, purification and adsorption efficiency is high;
  • 8.6. can be mixed to add a variety of, multi-layer adsorption materials.

Performance Highlight:

1.PLC control and touch screen operation: maximize artificial intelligence.

2. Automatic large transition cabin automatic pumping system: just simple operation in the touch screen.

3. Independent control cabinet internal integrated purification system: reduce the space occupied by the equipment at the same time, easy to move and replace, built-in 5Kg large-capacity organic solvent adsorption system (customized project), large-capacity professional-grade water, oxygen purification column adsorption system, can quickly purify the experimental environment inside the glove box. Under standard conditions, that is, 200C constant temperature, a standard atmospheric pressure, relative humidity 65%, 99.999% inert air source, water oxygen index is less than 1 ppm, and under normal circumstances, water oxygen index can reach less than 0.1 ppm.

Structural Highlight:

The front door can be opened with all-glass front window: the maximum convenience for the operator to access the enlarged object at any time.

Adjustable built-in tray: The operator can adjust the height of the tray up and down according to actual needs.

Basic Configuration:

NAMESERIAL NUMBERPARTUNITquantityQUANTITYOTHER
MAIN PART
1box bodypiece1 304 stainless steel thickness 3mm
2Transfer bunkerpiece1 304 stainless steel
3control systemcomplete set1

Germany SIEMENS

ABBelectron device

Import assembly
4gas recycle systemcomplete set1

Germany BASF

America UOPscavenging material

Germany BURKERT 

Import assembly
5display systemcomplete set1Germany SIEMENSImport
6glovepair1America PIERCANImport
7pipe jointcomplete set1  
8pressure gagepiece1Germany WIkaImport
9Water analyzerpiece1England MichellImport
10Oxygen analyzerpiece1Germany OEMImport
11vacuum pumppiece1England Edwards RV-12Import
12self-cleaningcomplete set1  
13Sound and light alarm systemcomplete set1  
14Organic solvent adsorption systemcomplete set1 customization
15Front door opencomplete set1  
16Automatic pumping and replenishing of transition bincomplete set1Germany BURKERTImport assembly

 

Remaining Configuration:

NAMESERIAL NUMBERSERIAL NUMBERUNITquantity生产商/品牌备注
Remaining Configuration
1Moving railcomplete set1HIWINTaiwan, CHINA
2PU gas pipe jointcomplete set1AIRTACTaiwan, CHINA
3Sealed silicone assemblycomplete set1 CHINA
4Stainless steel sleeve jointcomplete set1 CHINA
5Stainless steel precision steel pipecomplete set1 CHINA
6Precision copper tubecomplete set1 CHINA
7corrugated conduitcomplete set1 CHINA
8industrial castercomplete set1FOOTMASTERKorea

 

Technical Parameters:

  • 1. Box
  • 1.1. Box size: L x W x H =1220x 780 x 900mm.
  • 1.2. Material: All stainless steel structure (SUS 304), thickness 3mm.
  • 1.3. Glove mouth: diameter 220mm, hard aluminum alloy material, after anti-corrosion treatment.
  • 1.4. Gloves: American PIERCAN gloves, caliber 8 inches, thickness 0.4 mm, butyl rubber material.
  • 1.5. Window: Inclined design of the operating surface, using 10mm safety tempered glass, the front window and affixed with a special custom super sealing ring, using the front door open structure.
  • 1.6. A certain positive and negative pressure (-12mbar to 12mbar) can be maintained during use.
  • 1.7. The box is equipped with energy-saving lighting lamps and anti-reflective materials, which make the light soft and prevent visual fatigue.
  • 1.8. A perforated power terminal panel (Power supply: 220V±10% 50Hz±10%) is preset in the container.
  • 1.9. The box is equipped with 4 standard KF-40 interfaces for easy access to liquids, gases, signals, etc.
  • 1.10. The box is provided with 2 layers of storage boards, with upper and lower height adjustment function.
  • 1.11. Support: including casters, height 914mm. The caster has the functions of leveling, moving and fixing.
  • 1.12. Leakage rate: ≤0.05vol%/h. According to the ISO 10648-2 standard document clearly given the indicators:
  • The hourly leakage rate of the sealed box type with a controlled inert atmosphere is ≤5×.
  • 2. Transition cabin
  • Large transition module:
  • 2.1. Shape: Cylindrical (304 stainless steel), connected to the glove box, with automatic pumping air control.
  • 2.2. Size: Diameter 360mm, length 600mm large transition cabin (right operation), using gas spring type door opening mode, transition cabin with sliding tray.
  • 2.3. Large transition cabin tray: stainless steel 230mm ×595mm, can move freely around the extension depth of 361mm.
  • 2.4. Vacuum degree: ≤-0.1MPa(large transition chamber requires vacuum belt display), vacuum pressure gauge selected German Wika.
  • Small transition chamber:
  • 2.5. Shape: Cylindrical (304 stainless steel), connected to the glove box, controlled by a manual valve.
  • 2.6. Size: 150mm×300mm, single open handle pressing method.
  • 2.7. Vacuum degree: ≤-0.1MPa(small transition chamber requires vacuum belt display), vacuum pressure gauge selected German Wika.
  • 3. Control system
  • 3.1. Mode: Including self-diagnosis, power off self-start features, with pressure control and adaptive functions. Automatic control, cycle control, password protection, vacuum chamber control using LCD display. The control unit adopts German SIEMENS PLC touch screen, the operation menu is optional: Chinese/English.
  • 3.2. Pressure control: Control the pressure of the box and the transition chamber at a certain set value.
  • 3.3. Foot pedal: can control the pressure of the glove box, easy operation.
  • 4, circulation purification system
  • 4.1. Purification capacity: water, oxygen <0.1ppm.
  • 4.2. Adjustment device: The whole process of PLC touch adjustment (heating, evacuation, purification, regeneration) without human monitoring.
  • 4.3. Working gas: N2 or Ar (gas cycle).
  • 4.5. Circulation fan: Germany Elektror imported high-speed frequency conversion fan, flow 0-80m3/h, microprocessor control, pressure tested stainless steel device.
  • 4.6. Single purification column: Germany BASF deaeration material, the United States UOP high efficiency water absorption material, of which deaeration material 5kg, deaeration 60l, deaeration material 5kg, water removal 2kg.
  • 4.7. Purification valve: automatic electro-pneumatic valve. Modular design.
  • 4.8. Filter: High efficiency filter with HEPA standard 0.3 micron aperture filter.
  • 5. Regeneration system
  • It is used to reuse the purification system and activate it; Regeneration requires a mixture of N2/H2 or Ar/ H2 gases, with H2 accounting for 5-10%.
  • 6. Display system
  • Control unit adopts German SIEMENS PLC touch screen, operation menu: Chinese/English.
  • 7. Vacuum system
  • Automatic gas control plating plate; Vacuum pump selected British Edwards RV12 vacuum pump. The transition chamber can be vacuumed separately and can be controlled separately at any time. (Optional items)
  •  
  • Glove box selection configuration and main technical indicators
  • 1. Water analyzer
  • 1.1. Range: 0-1000ppm.
  • 1.2. Error: ±1% ppm.
  • 1.3. Environment: -10℃ -50 ℃.
  • 1.4. Display: PLC control display.
  • 1.5. especially for lithium battery manufacturing and metal-organic users, it can be cleaned and reused to avoid the problem of scrap after a pollution.
  • 2. Oxygen analyzer
  • 2.1. Range: 0-1000ppm.
  • 2.2. Error: ±1% ppm.
  • 2.3. Environment: -10℃ -50 ℃.
  • 2.4. Display: PLC control display.
  • 2.5The use of ZrO2 sensor avoids the problem that the fuel cell has a short life and cannot be exposed to the air.
  • 3, solvent adsorption system
  • 3.1. The effect of the agent on the purification column, the use of bypass system integrated into the glove box system, can effectively remove the solvent volatilized from the system, the media is mainly high quality and efficient activated carbon and activated alumina.
  • 3.2. Volume and weight of activated carbon cylinder Kg: 14.9L/5Kg

Basic Parameter:

  • 1. Net weight of glove box (Kg) : 555Kg.
  • 2. The net dimension of the glove box (mm) : length x width x height =2000 x 860 x 1860.
  • 3. Total power of the equipment: 0.8Kw.
  • 4. The internal strip provides power Kw: 2.5 Kw.

 

 

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